Ritonavir API Manufacturer in India

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Ritonavir API – Product Overview

Ritonavir is a synthetic HIV-1 protease inhibitor and antiretroviral active pharmaceutical ingredient. It is also widely used as a pharmacokinetic enhancer because of its potent inhibition of CYP3A-mediated drug metabolism. This pharmacokinetic-boosting property is particularly important when Ritonavir is administered with other antiviral agents.

Ritonavir has the molecular formula C₃₇H₄₈N₆O₅S₂ and a molecular weight of 720.94 g/mol. Its CAS Registry Number is 155213-67-5, and its FDA UNII is O3J8G9O825.

The current USP-NF monograph defines Ritonavir as containing 97.0–102.0%, calculated on the anhydrous basis.

Ritonavir API

Ritonavir is a structurally complex peptidomimetic molecule containing two thiazole rings, phenyl groups, multiple amide functionalities and several stereogenic centers. The API is produced as a defined stereochemical form, making stereochemical control an important part of its manufacturing and analytical quality strategy.

USP describes Ritonavir as a white-to-light-tan powder, while current U.S. labeling describes Ritonavir USP as white to almost white powder. It is freely soluble in methanol and methylene chloride, very slightly soluble in acetonitrile, and practically insoluble in water.

Ritonavir also exhibits polymorphism, making solid-state characterization important for pharmaceutical-grade API manufacture. WHO documentation notes that Ritonavir is described in the International Pharmacopoeia, Ph. Eur. and USP and has multiple crystal forms.

Chemical and Pharmaceutical Profile

PropertyDetails
API NameRitonavir
CAS Number155213-67-5
Molecular FormulaC₃₇H₄₈N₆O₅S₂
Molecular Weight720.94 g/mol
PubChem CID392622
FDA UNIIO3J8G9O825
ChEBI IDCHEBI:45409
API TypeSynthetic small-molecule API
Pharmacological ClassHIV protease inhibitor
Therapeutic ClassAntiretroviral
Physical FormWhite to light-tan / almost white powder
USP Assay97.0–102.0%, anhydrous basis
Water SolubilityPractically insoluble
Methanol SolubilityFreely soluble
Methylene Chloride SolubilityFreely soluble

Chemical identity and molecular information are supported by PubChem and USP.

Pharmaceutical Applications

Ritonavir is used in antiretroviral therapy and is particularly important as a pharmacokinetic enhancer for other antiviral medicines.

As an HIV protease inhibitor, Ritonavir inhibits the HIV protease enzyme required for processing viral polyproteins into mature functional proteins. However, at currently used low doses in combination regimens, its strong CYP3A inhibition is frequently exploited to increase systemic exposure to co-administered antiviral agents.

Ritonavir is included in several combination antiviral products. It is also used with nirmatrelvir in the treatment of COVID-19 in eligible patients under applicable regulatory indications. PubChem identifies Ritonavir as an HIV protease inhibitor and notes its use in combination with other antiviral agents.

Mechanism of Action

Ritonavir inhibits the HIV-1 protease enzyme, interfering with the cleavage of viral precursor polyproteins required for the production of mature infectious HIV particles.

Ritonavir also strongly inhibits CYP3A-mediated metabolism. This property can reduce the metabolism of co-administered drugs that are CYP3A substrates and thereby increase their plasma concentrations and duration of exposure.

This dual pharmacological profile explains the continuing importance of Ritonavir both as an antiretroviral agent and as a pharmacokinetic enhancer.

Quality and Analytical Testing

Ritonavir has an established USP-NF drug-substance monograph with detailed analytical requirements.

The current USP monograph specifies:

  • Assay: 97.0–102.0% on the anhydrous basis
  • Infrared identification
  • Chromatographic identification
  • Residue on ignition
  • Organic impurities by liquid chromatography
  • Water determination
  • Solid-state identification by X-ray diffraction where applicable

The USP assay uses liquid chromatography with UV detection at 240 nm. The monograph specifies system suitability requirements including column efficiency of NLT 5000 theoretical plates, tailing factor 0.8–1.2, and relative standard deviation NMT 2.0% for the assay system.

The current USP impurity section establishes NMT 0.1% for any other individual impurity and NMT 1.0% for total impurities, while several named Ritonavir-related impurities have specific limits of 0.1%, 0.2% or 0.3%.

Manufacturing

Ritonavir is manufactured through a controlled multi-step synthetic process requiring careful control of stereochemistry, intermediates, reaction conditions and process-related impurities.

The molecule contains multiple stereogenic centers, and selective production of the desired stereoisomer is important to API quality. WHO documentation specifically notes that Ritonavir has four chiral centres and that its manufacture stereoselectively produces the desired stereoisomer.

Manufacturing controls should include qualified raw materials, controlled reaction conditions, impurity monitoring, purification, crystallization, drying and appropriate solid-state characterization.

Physical and Physicochemical Properties

Ritonavir is a crystalline solid with a molecular weight of 720.94 g/mol. It is practically insoluble in water but has substantially greater solubility in organic solvents such as methanol and methylene chloride.

Ritonavir is also known to exhibit polymorphism. Solid-state form can therefore be relevant to API manufacturing, storage and pharmaceutical formulation. X-ray diffraction is included in the established USP identification approach for the drug substance when used for solid dosage forms.

Packaging and Storage

The USP monograph specifies that Ritonavir should be preserved in tight, light-resistant containers and stored between 5°C and 30°C.

Pharmaceutical-grade API should be packaged in suitable containers that protect the material from light, contamination and unsuitable environmental exposure. Packaging should maintain batch identification and traceability throughout storage and transportation.

Documentation

Pharmaceutical-grade Ritonavir API can be supported by appropriate quality and regulatory documentation, including:

  • Certificate of Analysis (CoA)
  • Safety Data Sheet (SDS)
  • API specification
  • USP compliance information
  • Analytical test methods
  • Related-substance profile
  • Residual-solvent information
  • Water-content information
  • Solid-state characterization
  • Stability data
  • GMP documentation
  • Technical and regulatory documentation, where applicable

Why Choose Ritonavir API Manufacturer in India?

Ritonavir is a highly established antiretroviral API with detailed pharmacopoeial requirements for identity, assay, impurities, water and solid-state quality.

A quality-focused Ritonavir API manufacturer in India should maintain appropriate stereochemical control, validated chromatographic methods, impurity management and solid-state characterization.

The USP-NF monograph provides particularly useful benchmarks, including the 97.0–102.0% anhydrous-basis assay, NMT 0.2% residue on ignition, NMT 0.5% water, NMT 0.1% any other individual impurity, and NMT 1.0% total impurities.

Detailed Specifications

Parameter Specification
Appearance white to off-white crystalline powder
Identification IR & HPLC compliant
Assay (HPLC) 97.0–102.0%
Residue on Ignition NMT 0.2%
Individual Impurity NMT 0.5%
Total Impurities NMT 1.0%
Water Content NMT 0.5%
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