Rilonacept API Manufacturer in India

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Rilonacept API Manufacturer in India

Rilonacept is a recombinant biological active pharmaceutical ingredient and a dimeric fusion protein that acts as an interleukin-1 cytokine trap. It consists of ligand-binding portions of the human interleukin-1 receptor component (IL-1R1) and interleukin-1 receptor accessory protein (IL-1RAcP), linked to the Fc portion of human IgG1. Rilonacept binds and neutralizes IL-1α and IL-1β, thereby inhibiting IL-1-mediated inflammatory signaling. 

Rilonacept is identified by CAS No. 501081-76-1, FDA UNII 8K80YB5GMG, and molecular weight of approximately 251 kDa. It is produced using recombinant Chinese hamster ovary (CHO) cells. 

Unlike conventional small-molecule APIs, Rilonacept is a complex recombinant protein. Therefore, conventional small-molecule parameters such as melting point, specific rotation, residue on ignition and simple HPLC assay are not appropriate primary quality specifications for the intact biological drug substance.

Rilonacept API

Rilonacept is an IL-1 inhibitor and recombinant fusion protein. It functions as a soluble decoy receptor that binds IL-1α and IL-1β and prevents their interaction with cell-surface IL-1 receptors. 

The current U.S. ARCALYST prescribing information describes Rilonacept as approximately 251 kDa and expressed in recombinant CHO cells. The finished product is supplied as a sterile white to off-white lyophilized powder. 

Chemical and Pharmaceutical Profile

ParameterDetails
Product NameRilonacept
SynonymsIL-1 Trap, Interleukin-1 Trap, IL-1-TRAP, KPL-914
CAS Number501081-76-1
FDA UNII8K80YB5GMG
DrugBankDB06372
ATC CodeL04AC04
API ClassRecombinant fusion protein / biological API
Molecular TypeDimeric Fc-fusion protein
Molecular WeightApproximately 251 kDa
Expression SystemRecombinant CHO cells
Protein ComponentsIL-1R1 ligand-binding domain + IL-1RAcP + human IgG1 Fc
TargetIL-1α and IL-1β
MechanismSoluble IL-1 cytokine trap
AppearanceWhite to off-white lyophilized powder
Reconstituted AppearanceClear, colorless to pale-yellow viscous solution
Finished Product Concentration80 mg/mL after reconstitution
Reconstituted pH6.5
Dosage FormLyophilized powder for solution for injection

The FDA label confirms the approximately 251 kDa molecular weight, CHO expression system, lyophilized appearance, 80 mg/mL reconstituted concentration and pH 6.5.

Pharmaceutical Applications

Rilonacept is used as an interleukin-1 inhibitor in inflammatory and autoinflammatory diseases.

Recurrent Pericarditis

Rilonacept is indicated for the treatment of recurrent pericarditis and reduction in the risk of recurrence in adults and pediatric patients 12 years and older. 

Cryopyrin-Associated Periodic Syndromes

Rilonacept is indicated for treatment of cryopyrin-associated periodic syndromes (CAPS), including:

  • Familial Cold Auto-inflammatory Syndrome (FCAS)
  • Muckle-Wells Syndrome (MWS)

These indications apply to adults and children 12 years and older under the current U.S. indication. 

Deficiency of Interleukin-1 Receptor Antagonist

Rilonacept is also indicated for maintenance of remission of Deficiency of Interleukin-1 Receptor Antagonist (DIRA) in adults and pediatric patients weighing 10 kg or more. 

Quality and Analytical Testing

Rilonacept requires a biological-product quality-control strategy rather than the conventional testing approach used for small-molecule APIs.

The EMA assessment report states that Rilonacept drug-substance specifications include controls for appearance, identification, strength, potency, purity and impurities

The EMA specifically states that Rilonacept drug-substance specifications include appearance, identification, strength, potency, purity and impurities. Public regulatory documents do not provide a complete set of numerical acceptance limits for every CMS field above. 

Important Biological API Testing

For Rilonacept, appropriate analytical characterization can include:

  • Protein identity
  • Peptide mapping
  • Intact molecular-weight determination
  • Purity and size variants
  • Aggregates
  • Fragmentation
  • Charge variants
  • Glycosylation characterization
  • Potency/binding activity
  • Host-cell protein
  • Host-cell DNA
  • Residual process-related impurities
  • Bioburden
  • Endotoxin
  • Sterility where applicable
  • Protein concentration
  • pH
  • Osmolality where applicable
  • Stability-indicating studies

These tests are more scientifically appropriate for Rilonacept than conventional small-molecule API tests such as melting point or residue on ignition.

Rilonacept API Manufacturer in India

Rilonacept manufacturing requires recombinant protein production using a suitable mammalian expression system followed by purification, formulation and extensive biological characterization.

The FDA identifies recombinant CHO cells as the production system for Rilonacept. 

Important manufacturing and quality controls include:

  • Recombinant CHO-cell production
  • Controlled cell culture
  • Harvest and clarification
  • Protein purification
  • Viral safety controls
  • Protein identity
  • Molecular-weight characterization
  • Purity and aggregate control
  • Charge-variant control
  • Glycosylation characterization
  • Potency testing
  • Host-cell protein testing
  • Host-cell DNA testing
  • Residual process impurity testing
  • Sterility/bioburden controls
  • Endotoxin testing
  • Stability testing

The EMA assessment concluded that the proposed Rilonacept drug-substance specifications covered the relevant quality attributes, including appearance, identity, strength, potency, purity and impurities.

Detailed Specifications

Parameter Specification
Appearance white to off-white crystalline powder
Identification IR & HPLC compliant
Assay (HPLC) 98.0% – 102.0%
pH (1% Solution) 6.5
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