Rifapentine API Manufacturer in India

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Rifapentine API Manufacturer in India

Rifapentine is a semisynthetic rifamycin-class antimycobacterial active pharmaceutical ingredient used in pharmaceutical formulations for the treatment of tuberculosis and latent tuberculosis infection. It inhibits bacterial DNA-dependent RNA polymerase and interferes with bacterial RNA synthesis.

Rifapentine is identified by CAS No. 61379-65-5, molecular formula C₄₇H₆₄N₄O₁₂, and molecular weight approximately 877.04 g/mol. It is also identified by FDA UNII XJM390A33U, ChEBI CHEBI:45304, and DrugBank DB01201.

WHO lists Rifapentine as a prequalified active pharmaceutical ingredient, with Lupin Ltd. listed as an assessed API manufacturer.

Rifapentine API

Rifapentine belongs to the rifamycin/ansamycin antibiotic class and is structurally related to rifampicin while having a cyclopentyl-substituted piperazine side chain.

The API is generally described as a red to brown or reddish crystalline powder. It has very low aqueous solubility, making solid-state characteristics and particle-size control important considerations during pharmaceutical manufacturing. WHO's assessment of Rifapentine-containing products specifically considers the API's physicochemical and quality characteristics.

Rifapentine is used in combination with other anti-tuberculosis medicines rather than as monotherapy for active TB.

Chemical and Pharmaceutical Profile

ParameterDetails
Product NameRifapentine
SynonymsPriftin, Rifapentin, Cyclopentylrifampicin, Rifamycin AF/ACPP, MDL 473
CAS Number61379-65-5
Molecular FormulaC₄₇H₆₄N₄O₁₂
Molecular Weight877.04 g/mol
FDA UNIIXJM390A33U
ChEBICHEBI:45304
DrugBankDB01201
ATC CodeJ04AB05
API ClassRifamycin / Ansamycin antibiotic
Therapeutic ClassAntimycobacterial
AppearanceRed to brown / reddish crystalline powder
Water SolubilityPractically insoluble / very slightly soluble
Melting Point174°C reference value
Maximum Absorption475 nm reference value
Storage ReferenceProtect from moisture and heat; validated API stability conditions apply

PubChem confirms the identity, CAS number, molecular formula, molecular weight and major identifiers. TCI reports a reference melting point of 174°C and maximum absorption wavelength of 475 nm.

Pharmaceutical Applications

Rifapentine API is primarily used in pharmaceutical products intended for tuberculosis management.

Active Tuberculosis

Rifapentine is used in combination with other antimycobacterial medicines for the treatment of active tuberculosis caused by susceptible Mycobacterium tuberculosis.

Latent Tuberculosis Infection

Rifapentine is also used in combination treatment regimens for latent tuberculosis infection to reduce the risk of progression to active TB.

Pharmaceutical Formulations

Rifapentine API is used for the manufacture of:

  • Rifapentine tablets
  • Rifapentine dispersible tablets
  • Isoniazid/Rifapentine combination tablets
  • Other approved tuberculosis combination formulations

WHO currently lists prequalified Rifapentine 150 mg dispersible tablets and Isoniazid/Rifapentine products.

Quality and Analytical Testing

Rifapentine requires comprehensive pharmaceutical quality control covering identification, assay, related substances, water content, residual solvents, physical properties and solid-state characteristics

The numerical values marked with an asterisk are published commercial/CP specifications and should not be presented as a universal USP specification. WHO confirms that accepted API specifications exist but notes that the accepted detailed specification and analytical methods may be provided through the API manufacturer rather than fully disclosed publicly.

TCI currently reports minimum 98.0 area% HPLC purity, minimum 97.0% nonaqueous titration, and a reference melting point of 174°C.

Important Analytical Parameters

Rifapentine quality control can include:

  • IR identification
  • HPLC identification
  • UV identification
  • HPLC assay
  • Related substances
  • Water determination
  • Residue on ignition
  • Heavy-metal/elemental impurity control
  • Residual solvents
  • Polymorphic-form characterization
  • Particle-size distribution
  • Microbial quality
  • Stability testing

A recent 2026 stability-indicating LC method for Rifapentine reported HPLC assay results and validated impurity detection at low levels, supporting the use of chromatographic impurity profiling for routine quality control.

Rifapentine API Manufacturer in India

Rifapentine API manufacturing requires controlled synthesis, purification and pharmaceutical quality testing because of the molecule's complex rifamycin structure and physicochemical characteristics.

Important manufacturing controls include:

  • Controlled synthetic process
  • Purification and crystallization
  • HPLC assay
  • Related-substance profiling
  • IR/UV identity testing
  • Water-content determination
  • Residue-on-ignition testing
  • Residual-solvent testing
  • Elemental impurity assessment
  • Particle-size control
  • Solid-state/polymorph characterization
  • Stability testing
  • Batch-to-batch consistency

WHO's API prequalification list currently identifies Lupin Ltd. as a prequalified Rifapentine API applicant, with the API prequalification dated 10 June 2024 and confirmation dated 29 April 2026.

WHO also identifies Indian Rifapentine API manufacturing sites associated with prequalified products, including sites of Lupin and Macleods.

Packaging and Storage

Rifapentine API should be stored in suitable pharmaceutical-grade, well-closed packaging that protects the material from moisture, light and excessive heat.

Commercial reference material from TCI is stored frozen at −20°C under inert gas and is identified as moisture- and heat-sensitive. This is a commercial reference-material condition and should not automatically be used as the universal pharmaceutical API storage condition.

For finished Rifapentine pharmaceutical products, WHO-prequalified products are stored not above 30°C and protected from moisture.

Packaging Considerations

  • Double polyethylene-lined pharmaceutical bags
  • Suitable HDPE/fiber drums or validated containers
  • Moisture-protective packaging
  • Light protection where required
  • Tight closure
  • Batch identification and traceability
  • Storage according to validated stability data

Documentation

Typical Rifapentine API documentation may include:

  • Certificate of Analysis (CoA)
  • Certificate of Origin (CoO)
  • Safety Data Sheet (SDS)
  • Product Specification
  • Analytical Test Methods
  • HPLC Assay Report
  • Related Substance Chromatograms
  • IR Spectrum
  • UV Spectrum
  • Water Content Report
  • Residual Solvent Report
  • Residue on Ignition Report
  • Heavy Metal / Elemental Impurity Data
  • Particle Size Distribution
  • Polymorphism / Solid-State Data
  • Stability Data
  • Microbial Test Report
  • GMP Documentation
  • Regulatory Support Documentation
  • Batch Manufacturing Documentation
  • Traceability Documentation

Detailed Specifications

Parameter Specification
Appearance white to off-white crystalline powder
Identification IR & HPLC compliant
Assay (HPLC) 98.0% – 102.0%
Residue on Ignition NMT 0.20%
Heavy Metals NMT 20 ppm
Individual Impurity NMT 1.0%
Total Impurities NMT 3.0%
Water Content NMT 5.0%
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