Remibrutinib API Manufacturer in India

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Remibrutinib is an orally active, selective Bruton’s tyrosine kinase (BTK) inhibitor developed for the treatment of chronic spontaneous urticaria (CSU). It is a small-molecule kinase inhibitor and is marketed in the United States as Rhapsido.

The FDA approved remibrutinib in 2025 for adults with chronic spontaneous urticaria who remain symptomatic despite H1-antihistamine treatment. The approved dosage is 25 mg twice daily.

Remibrutinib has the molecular formula C₂₇H₂₇F₂N₅O₃, molecular weight 507.54 g/mol, and CAS Registry Number 1787294-07-8.

API / Product Information

ParameterDetails
Product NameRemibrutinib
CAS Number1787294-07-8
PubChem CID118107483
FDA UNIII7MVZ8HDNU
ChEMBL IDCHEMBL4483575
DrugBank IDDB16852
KEGG IDD12285
Molecular FormulaC₂₇H₂₇F₂N₅O₃
Molecular Weight507.54 g/mol
Drug ClassBTK inhibitor
Therapeutic ClassImmunomodulatory / antiallergic
RouteOral
Approved Strength25 mg tablet
Primary TargetBruton’s tyrosine kinase (BTK)

FDA identifies remibrutinib as a kinase inhibitor with a molecular weight of approximately 507.54 g/mol.

Chemical and Pharmaceutical Profile

The chemical name of remibrutinib is:

N-(3-{6-Amino-5-[2-(N-methylprop-2-enamido)ethoxy]pyrimidin-4-yl}-5-fluoro-2-methylphenyl)-4-cyclopropyl-2-fluorobenzamide

Its molecular formula is C₂₇H₂₇F₂N₅O₃. PubChem reports a molecular weight of 507.5 g/mol, while the FDA label gives approximately 507.54 g/mol.

Selected physicochemical descriptors from PubChem include:

  • Molecular formula: C₂₇H₂₇F₂N₅O₃
  • Molecular weight: 507.5 g/mol
  • Exact mass: approximately 507.2218 Da
  • XLogP3-AA: approximately 2.2
  • Hydrogen-bond donors: 3
  • Hydrogen-bond acceptors: 8
  • Rotatable bonds: 10
  • Topological polar surface area: approximately 115 Ų
  • Formal charge: 0

 

Pharmaceutical Applications

Remibrutinib is approved for the treatment of chronic spontaneous urticaria (CSU) in adults who remain symptomatic despite H1-antihistamine treatment.

The approved U.S. product is supplied as 25 mg film-coated tablets, administered orally twice daily. The FDA review identifies a maximum daily dose of 50 mg.

Remibrutinib has also been investigated in other immune-mediated and inflammatory disorders, but these investigational applications should not be represented as approved indications.

Mechanism of Action

Remibrutinib is a selective BTK inhibitor. Bruton’s tyrosine kinase participates in intracellular signaling downstream of the FcεRI, Fcγ receptors and B-cell receptor (BCR) pathways.

By inhibiting BTK, remibrutinib suppresses signaling involved in activation and degranulation of mast cells and basophils and reduces release of histamine and other inflammatory mediators involved in urticaria.

FDA notes that remibrutinib also inhibits the related kinases TEC and BMX.

Quality and Analytical Testing

Remibrutinib is a synthetic small-molecule API and requires conventional pharmaceutical chemical characterization.

Appropriate quality testing includes:

  • Identification by IR spectroscopy
  • Identification by XRPD
  • HPLC assay
  • Related substances by HPLC
  • Specific impurity testing
  • Residual solvents by GC
  • Water content by Karl Fischer
  • Sulphated ash
  • Elemental impurity assessment
  • Particle-size distribution
  • Microbiological quality
  • Stability-indicating testing

The EMA assessment report specifically states that the active-substance specification includes appearance, particle size, IR, XRPD, related substances by HPLC, residual solvents, water by Karl Fischer, sulphated ash, phosphorus content by ICP-OES, specific GC/HPLC-MS impurities, assay on anhydrous and solvent-free basis, and microbiological testing.

Manufacturing

Remibrutinib is a synthetic small-molecule pharmaceutical API manufactured through controlled chemical synthesis followed by purification and isolation.

Manufacturing controls should cover:

  • Qualified starting materials
  • Controlled reaction conditions
  • Intermediate purity
  • Process-related impurities
  • Degradation products
  • Residual solvents
  • Solid-state properties
  • Particle-size distribution
  • Final assay
  • Stability
  • Packaging integrity

The regulatory assessment reports that commercial-scale batches were consistent with the proposed specification and that the active substance manufacturing process had demonstrated acceptable control.

Physical and Physicochemical Properties

PropertyValue
Molecular FormulaC₂₇H₂₇F₂N₅O₃
Molecular Weight507.54 g/mol
Exact Mass~507.2218 Da
H-Bond Donors3
H-Bond Acceptors8
Rotatable Bonds10
TPSA~115 Ų
Formal Charge0
Physical FormWhite to pale yellow powder
Water SolubilityPractically insoluble according to FDA labeling
Stereocenters0

FDA describes remibrutinib as a white to pale yellow powder that is practically insoluble in water.

The FDA review further describes remibrutinib as a weak base with high permeability and low solubility at physiological pH and classifies it as BCS Class 2.

Packaging and Storage

The active substance is packaged in a pharmaceutical-grade containment system. The EMA assessment describes LDPE bags placed inside triple-laminated foil bags, with the bags stored in drums for handling and transportation.

For the marketed finished product, FDA specifies storage at 20°C to 25°C, with excursions permitted between 15°C and 30°C. The product should remain in its original packaging to protect it from moisture.

Bulk API storage should follow the validated API stability program and approved storage specification.

Documentation

Typical documentation for pharmaceutical-grade Remibrutinib API may include:

  • Certificate of Analysis (CoA)
  • Certificate of Conformance
  • Safety Data Sheet (SDS)
  • Product specification
  • Analytical method information
  • Stability data
  • Related-substance profile
  • Residual-solvent data
  • Particle-size data
  • Solid-state characterization
  • Elemental impurity assessment
  • Manufacturing documentation
  • Regulatory documentation, where applicable

Why Choose Remibrutinib API Manufacturer in India

A qualified Remibrutinib API manufacturing program should emphasize controlled chemical synthesis, impurity management and consistent solid-state quality.

Important quality considerations include:

  • Controlled synthetic manufacturing
  • High API purity
  • Validated HPLC methods
  • Related-substance control
  • Residual-solvent control
  • Water-content control
  • Particle-size control
  • Solid-state characterization
  • Batch-to-batch consistency
  • Stability monitoring
  • Pharmaceutical-grade packaging
  • Comprehensive quality documentation

Detailed Specifications

Parameter Specification
Appearance white to off-white crystalline powder
Identification IR & HPLC compliant
Assay (HPLC) 98.0% – 102.0%
Loss on Drying NMT 0.5%
Residue on Ignition NMT 0.1%
Heavy Metals NMT 20 ppm
Individual Impurity NMT 0.10%
Total Impurities NMT 0.50%
Water Content NMT 1.0%
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