Rabeprazole Sodium API Manufacturer in India

Swapnroop Pharma · WHO-GMP Certified · +91 87670 62101

Product Overview

Rabeprazole Sodium is the sodium salt of rabeprazole, a substituted benzimidazole proton-pump inhibitor (PPI). It suppresses gastric acid secretion by inhibiting the gastric H⁺/K⁺-ATPase proton pump located on the secretory surface of gastric parietal cells. (dailymed.nlm.nih.gov)

Rabeprazole Sodium is used as an active pharmaceutical ingredient in delayed-release oral formulations for acid-related gastrointestinal disorders. The API is chemically sensitive to acidic conditions and is more stable under alkaline conditions. (dailymed.nlm.nih.gov)

The anhydrous form has the molecular formula C₁₈H₂₀N₃NaO₃S and molecular weight 381.42 g/mol. The USP specification also recognizes hydrated forms separately. (pubchem.ncbi.nlm.nih.gov)

Chemical Characteristics

  • Product Name: Rabeprazole Sodium
  • CAS Number: 117976-90-6
  • Molecular Formula: C₁₈H₂₀N₃NaO₃S
  • Molecular Weight: 381.42 g/mol
  • PubChem CID: 14720269
  • UNII: 3L36P16U4R
  • ChEBI ID: CHEBI:8769
  • EC Number: 629-730-3
  • Active Moiety: Rabeprazole
  • Salt Form: Sodium salt
  • IUPAC Name: Sodium 2-[[4-(3-methoxypropoxy)-3-methyl-2-pyridinyl]methylsulfinyl]benzimidazol-1-ide
  • InChIKey: KRCQSTCYZUOBHN-UHFFFAOYSA-N
  • Exact Mass: 381.11230696 Da
  • H-Bond Donors: 0
  • H-Bond Acceptors: 7
  • Rotatable Bonds: 8
  • TPSA: 81.5 Ų

PubChem confirms CAS 117976-90-6, formula C₁₈H₂₀N₃NaO₃S and molecular weight 381.4 g/mol. (pubchem.ncbi.nlm.nih.gov)

Pharmacological Class

Rabeprazole Sodium belongs to the proton-pump inhibitor (PPI) class and is classified as a substituted benzimidazole antisecretory compound.

Mechanism of Action

Rabeprazole is protonated and accumulated within the acidic environment of gastric parietal cells, where it is converted into an active sulfenamide. The active form binds to and inhibits the H⁺/K⁺-ATPase, blocking the final step of gastric acid secretion. (dailymed.nlm.nih.gov)

The pharmacodynamic effect is prolonged because inhibition of the proton pump persists beyond the relatively short plasma half-life of rabeprazole.

Pharmaceutical Applications

Rabeprazole Sodium API is used in pharmaceutical formulations for acid-related gastrointestinal conditions, including:

  • Gastroesophageal reflux disease (GERD)
  • Healing and maintenance of erosive or ulcerative GERD
  • Duodenal ulcers
  • Gastric acid hypersecretory conditions such as Zollinger-Ellison syndrome
  • Combination therapy for Helicobacter pylori eradication

U.S. labeling includes delayed-release rabeprazole sodium tablets for GERD, duodenal ulcer treatment and pathological hypersecretory conditions, with combination therapy used for H. pylori eradication. (dailymed.nlm.nih.gov)

Physical and Physicochemical Properties

Rabeprazole Sodium is described as a white to off-white, hygroscopic powder. It is freely soluble in methanol and methylene chloride. Its stability is strongly pH-dependent: it is rapidly degraded in acidic media and is more stable under alkaline conditions. (dailymed.nlm.nih.gov)

PropertyValue
Molecular Weight381.42 g/mol
Exact Mass381.11230696 Da
H-Bond Donors0
H-Bond Acceptors7
Rotatable Bonds8
TPSA81.5 Ų
Physical FormWhite to off-white hygroscopic powder

(pubchem.ncbi.nlm.nih.gov)

Analytical Profile

Rabeprazole Sodium API can be characterized using:

  • HPLC/UPLC assay
  • HPLC related-substance analysis
  • UV spectroscopy
  • IR spectroscopy
  • LC-MS
  • NMR spectroscopy
  • Water determination
  • Loss-on-drying testing
  • Residual-solvent analysis
  • Elemental impurity testing

The USP monograph includes IR identification, sodium identification, assay, organic-impurity testing and specific tests for loss on drying or water depending on whether the material is anhydrous or hydrated. (turn1search0)

API Quality and Impurity Control

The current USP 2025 information identifies Rabeprazole Sodium as containing NLT 98.0% and NMT 102.0% of rabeprazole sodium, calculated on the dried basis for the anhydrous form and on the anhydrous basis for the hydrated form. (turn1search0)

The USP specification also controls organic impurities. A published USP specification identifies a total impurities limit of NMT 1.0%. (turn1search38)

The principal impurity/reference standards include Rabeprazole Related Compounds A, B, C, D, E and F, covering degradation and process-related substances such as the N-oxide, sulfide and sulfone analogues. (turn1search0)

Stereochemical Characteristics

The standard Rabeprazole Sodium record represents the sodium salt without a defined stereochemical center. However, (S)-Rabeprazole Sodium is separately identified as a stereochemically defined material, with molecular formula C₁₈H₂₁N₃NaO₃S and molecular weight 382.4 g/mol. (pubchem.ncbi.nlm.nih.gov)

Therefore, the API specification should clearly identify whether the material is the standard racemic/unspecified stereochemical form or a specifically controlled stereoisomer.

Storage and Handling

Rabeprazole Sodium should be protected from conditions that promote degradation. Current labeling describes the material as hygroscopic and pH-sensitive, with greater stability under alkaline conditions. (dailymed.nlm.nih.gov)

The USP information specifies:

  • Preserve in tight containers.
  • Store at room temperature.
  • Hydrated material should be identified and controlled as the appropriate hydrated form. (turn1search0)

Documentation

Typical Rabeprazole Sodium API documentation may include:

  • Certificate of Analysis (CoA)
  • Safety Data Sheet (SDS)
  • HPLC assay chromatogram
  • Related-substance chromatogram
  • IR spectrum
  • LC-MS data
  • NMR data
  • Loss-on-drying report
  • Water-content report
  • Residual-solvent report
  • Elemental impurity data
  • Stability data
  • Batch analytical report
  • Pharmacopoeial compliance statement

Pharmaceutical API Manufacturing

Rabeprazole Sodium API manufacturing requires controlled synthesis, purification, sodium-salt formation, drying and analytical testing.

Particular attention should be given to chemical purity, organic impurities, moisture/hydration state, hygroscopicity and stability under acidic conditions. The final API should comply with the applicable current USP or registered specification.

Detailed Specifications

Parameter Specification
Appearance white to off-white crystalline powder
Identification IR & HPLC compliant
Assay (HPLC) 98.0% – 102.0%
Loss on Drying NMT 0.5%
Residue on Ignition NMT 0.1%
Individual Impurity NMT 0.5%
Total Impurities NMT 1.0%
Water Content NMT 7.0%
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