Pyrimethamine API Manufacturer in India

Swapnroop Pharma · WHO-GMP Certified · +91 87670 62101

Product Overview

Pyrimethamine is a synthetic antiprotozoal and antimalarial API belonging to the aminopyrimidine class. It acts primarily as an inhibitor of dihydrofolate reductase (DHFR) and interferes with folate metabolism in susceptible protozoa.

Pyrimethamine is used principally in combination regimens for the treatment of toxoplasmosis and certain other protozoal infections. It has also historically been used as an antimalarial, although resistance has limited its use as a standalone malaria treatment. PubChem identifies pyrimethamine as an aminopyrimidine, antiprotozoal, antimalarial and DHFR inhibitor.

Chemical Characteristics

  • Product Name: Pyrimethamine
  • CAS Number: 58-14-0
  • Molecular Formula: C₁₂H₁₃ClN₄
  • Molecular Weight: 248.71 g/mol
  • PubChem CID: 4993
  • UNII: Z3614QOX8W
  • EC Number: 200-364-2
  • IUPAC Name: 5-(4-chlorophenyl)-6-ethylpyrimidine-2,4-diamine
  • InChIKey: WKSAUQYGYAYLPV-UHFFFAOYSA-N
  • Exact Mass: 248.0828741 Da
  • XLogP3: 2.7
  • Hydrogen Bond Donors: 2
  • Hydrogen Bond Acceptors: 4
  • Rotatable Bonds: 2
  • Topological Polar Surface Area: 77.8 Ų

The molecular identity and numerical physicochemical data are supported by PubChem and NIST.

Pharmacological Class

Pyrimethamine belongs to the aminopyrimidine antiprotozoal class and functions as a dihydrofolate reductase inhibitor.

Mechanism of Action

Pyrimethamine inhibits the enzyme dihydrofolate reductase (DHFR) in susceptible protozoa. Inhibition of DHFR interferes with the conversion of dihydrofolate to tetrahydrofolate, reducing the availability of folate derivatives required for nucleotide synthesis and cellular replication.

This antifolate mechanism contributes to its antiprotozoal activity and is particularly relevant to treatment of Toxoplasma gondii infections.

Pharmaceutical Applications

Pyrimethamine API is used in pharmaceutical formulations and combination therapies for:

  • Toxoplasmosis
  • Protozoal infections
  • Selected antimalarial applications
  • Combination therapy with sulfonamides
  • Pharmaceutical research and development

Pyrimethamine is commonly used with leucovorin (folinic acid) to reduce toxicity associated with folate antagonism. PubChem identifies its use as an antimalarial and in combination with a sulfonamide for toxoplasmosis.

Physical Properties

Pyrimethamine is described as an odorless, white crystalline powder.

NIST confirms a molecular weight of 248.711 g/mol and CAS number 58-14-0.

A reported melting range for pyrimethamine is approximately 233–234°C. Because melting-point values can vary with measurement method and material form, this value should be treated as a reference physical property rather than an API release specification.

Physicochemical Characteristics

PropertyValue
Molecular Weight248.71 g/mol
Exact Mass248.0828741 Da
XLogP32.7
H-Bond Donors2
H-Bond Acceptors4
Rotatable Bonds2
TPSA77.8 Ų
Melting PointApprox. 233–234°C

PubChem reports the calculated molecular descriptors, while NIST provides the molecular formula and molecular weight.

Analytical Profile

Pyrimethamine API can be characterized using:

  • HPLC/UPLC assay
  • Related-substance analysis
  • UV spectroscopy
  • IR spectroscopy
  • NMR spectroscopy
  • Mass spectrometry
  • Residual-solvent analysis
  • Water-content determination
  • Elemental impurity analysis

Chromatographic testing is particularly important for determining assay, degradation products and process-related impurities.

API Quality and Impurity Control

Quality control for Pyrimethamine API should address:

  • Identification
  • Assay
  • Related substances
  • Degradation products
  • Residual solvents
  • Water content
  • Elemental impurities
  • Appearance
  • Microbiological quality where applicable

Pyrimethamine is listed in PubChem with references to USP and WHO International Pharmacopoeia monographs, indicating established pharmacopoeial recognition.

Specific numerical acceptance limits should be taken from the applicable current pharmacopoeial monograph or registered API specification rather than using unsupported generic limits.

Stereochemical Characteristics

Pyrimethamine contains no stereogenic center in its standard chemical structure. Therefore, stereochemical/chiral purity is not applicable as a routine API specification.

Storage and Handling

Pyrimethamine should be stored according to the applicable pharmacopoeial and approved API stability requirements.

Recommended handling practices include:

  • Keep in a tightly closed container.
  • Protect from excessive moisture.
  • Protect from direct light where required.
  • Avoid unnecessary exposure to heat.
  • Handle according to the applicable SDS.
  • Use validated storage conditions established through stability studies.

Documentation

Typical pharmaceutical API documentation may include:

  • Certificate of Analysis (CoA)
  • Safety Data Sheet (SDS)
  • HPLC chromatogram
  • Related-substance chromatogram
  • IR spectrum
  • NMR data
  • Residual-solvent report
  • Water-content report
  • Elemental impurity data
  • Stability data
  • Batch analytical report
  • Regulatory documentation where applicable

Pharmaceutical API Manufacturing

Pyrimethamine API manufacturing involves controlled synthesis, purification, isolation, drying and analytical testing. Critical quality attributes include chemical identity, assay, related substances, residual solvents and physical characteristics.

The finished API should comply with the applicable current pharmacopoeial or registered specification.

Detailed Specifications

Parameter Specification
Appearance white to off-white crystalline powder
Identification IR & HPLC compliant
Assay (HPLC) 98.0% – 102.0%
Loss on Drying NMT 0.5%
Residue on Ignition NMT 0.1%
Melting Point Approx. 233–234°C reference value
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