Oxaprozin API Manufacturer in India

Swapnroop Pharma · WHO-GMP Certified · +91 87670 62101

Product Overview

Oxaprozin is a nonsteroidal anti-inflammatory drug (NSAID) belonging to the propionic acid derivative class. Chemically, it is known as 4,5-diphenyl-2-oxazolepropionic acid and is used for its anti-inflammatory, analgesic and antipyretic properties.

Oxaprozin is a well-characterized small-molecule pharmaceutical API with the molecular formula C18H15NO3 and molecular weight 293.32 g/mol. It is described as a white to off-white or yellowish-white crystalline powder and has a reported melting range of approximately 162–163°C.

The current publicly reproduced USP 2025 monograph specifies 98.0–102.0% oxaprozin on the dried basis, together with numerical requirements for residue on ignition, arsenic, organic impurities and loss on drying.

Chemical Information

  • Product Name: Oxaprozin
  • Chemical Name: 4,5-Diphenyl-2-oxazolepropionic acid
  • CAS Number: 21256-18-8
  • UNII: MHJ80W9LRB
  • Molecular Formula: C18H15NO3
  • Molecular Weight: 293.32 g/mol
  • Exact Mass: 293.1052 Da
  • Chemical Class: Oxazole derivative
  • Therapeutic Class: NSAID
  • Pharmacological Class: Nonsteroidal anti-inflammatory agent
  • Stereochemistry: Achiral
  • Physical Form: Crystalline powder
  • Appearance: White to off-white / yellowish-white crystalline powder
  • pKa: 4.3
  • Log P: 4.8 at physiological pH
  • Melting Point: 162–163°C

The chemical identity and molecular data are supported by PubChem and FDA/DailyMed information.

Mechanism of Action

Oxaprozin produces analgesic, anti-inflammatory and antipyretic effects primarily through inhibition of prostaglandin synthesis.

  • Oxaprozin inhibits cyclooxygenase-related prostaglandin synthesis.
  • It reduces the formation of prostaglandin mediators involved in inflammation and pain.
  • Reduced prostaglandin production decreases inflammatory responses and pain sensitization.
  • Its pharmacological activity is consistent with other NSAIDs, although its precise mechanism is not completely understood.
  • Oxaprozin has activity against pathways involving both COX-1 and COX-2.

FDA labeling describes oxaprozin as a potent inhibitor of prostaglandin synthesis and attributes its mechanism to cyclooxygenase/prostaglandin-synthesis inhibition.

Key Features

  • Pharmaceutical-grade Oxaprozin API
  • NSAID pharmaceutical active ingredient
  • CAS 21256-18-8
  • Molecular formula C18H15NO3
  • Molecular weight 293.32 g/mol
  • USP monograph available
  • USP assay requirement 98.0–102.0%
  • Loss on drying NMT 0.3%
  • Residue on ignition NMT 0.3%
  • Arsenic NMT 1 ppm
  • Heavy metals 0.001% / 10 ppm in the earlier USP specification
  • Current USP organic impurity limits include NMT 0.10% for multiple specified impurities
  • Total impurities NMT 0.5%
  • White to off-white crystalline powder
  • Melting point approximately 162–163°C
  • Practically insoluble in water
  • Slightly soluble in alcohol
  • Light-sensitive API requiring light-resistant packaging

The current USP 2025 reproduction specifies 98.0–102.0% assay and detailed organic impurity controls.

Pharmaceutical Applications

Oxaprozin API is used in pharmaceutical development and manufacturing of NSAID products intended for management of inflammatory and painful musculoskeletal conditions.

Applications include:

  • Osteoarthritis formulations
  • Rheumatoid arthritis formulations
  • Anti-inflammatory pharmaceutical development
  • Analgesic formulations
  • NSAID research
  • Pharmaceutical formulation development
  • Analytical reference-standard applications
  • Stability and degradation studies
  • Related-substance method development

FDA labeling identifies oxaprozin as an NSAID used for the relief of signs and symptoms associated with osteoarthritis and rheumatoid arthritis.

Physicochemical Properties

Oxaprozin is a crystalline, aromatic oxazole-containing propionic acid derivative.

  • Appearance: White to off-white / yellowish-white crystalline powder
  • Molecular Weight: 293.32 g/mol
  • Melting Point: 162–163°C
  • pKa: 4.3
  • Log P: 4.8 at pH 7.4
  • Water Solubility: Practically insoluble / insoluble
  • Alcohol Solubility: Slightly soluble
  • Methanol: Sparingly soluble
  • Ethanol: Sparingly soluble
  • Ether: Slightly soluble

FDA/DailyMed describes oxaprozin as slightly soluble in alcohol and insoluble in water, while another USP product description reports it as sparingly soluble in methanol and ethanol, slightly soluble in ether and practically insoluble in water.

Analytical Characterization

Oxaprozin has a well-defined USP analytical profile.

Identification

USP identification uses:

  • Infrared absorption spectroscopy
  • HPLC retention-time comparison
  • UV absorption characterization

The USP identification procedure includes comparison of the oxaprozin HPLC retention time with the reference standard. The UV identification in the earlier monograph specifies an absorbance at 285 nm of 0.455–0.495 using a 10 µg/mL methanolic solution.

Assay

The current USP 2025 monograph uses liquid chromatography for assay.

Key parameters include:

  • Detector: UV
  • Wavelength: 285 nm
  • Column: 4.6 mm × 15 cm
  • Particle size: 5 µm
  • Packing: L7
  • Column temperature: 25°C
  • Flow rate: 1.0 mL/min
  • Injection volume: 20 µL
  • Assay: 98.0–102.0% on dried basis

System suitability includes a tailing factor of NMT 2.0 and relative standard deviation of NMT 0.73%.

Organic Impurity Profile

The current USP 2025 monograph provides specific numerical controls for oxaprozin-related impurities.

Specified impurities include:

  • Oxaprozin imidazole analog — NMT 0.10%
  • Benzoin — NMT 0.10%
  • Oxaprozin amide — NMT 0.10%
  • Benzoin succinate — NMT 0.10%
  • Benzil — NMT 0.10%
  • Oxaprozin bisoxazole analog — NMT 0.10%
  • Tetraphenylpyrazine — NMT 0.10%
  • Individual unspecified impurity — NMT 0.06%
  • Total impurities — NMT 0.50%
  • Reporting threshold — 0.03%

These are particularly valuable CMS values because they come from the current USP 2025 monograph reproduction rather than generic API assumptions.

Inorganic Impurities

The USP monograph includes controls for inorganic impurities.

  • Residue on ignition: NMT 0.3%
  • Arsenic: NMT 1 ppm
  • Heavy metals: 0.001%, equivalent to 10 ppm, in the earlier USP specification

The current USP 2025 text specifically retains the arsenic limit of NMT 1 ppm and residue-on-ignition limit of NMT 0.3%.

Loss on Drying

Oxaprozin is tested by loss on drying:

  • Temperature: 105°C
  • Duration: 2 hours
  • Acceptance criterion: NMT 0.3%

The current USP 2025 monograph specifies NMT 0.3% loss on drying.

Light Sensitivity

Oxaprozin is described as light sensitive. The USP monograph specifically instructs that Oxaprozin samples and standard solutions should be protected from light and recommends tight, light-resistant containers for storage.

Quality and Regulatory Information

Oxaprozin has a USP monograph and is therefore substantially better defined from a public compendial perspective than many newer pharmaceutical APIs.

Quality testing can include:

  • Identification
  • HPLC assay
  • Organic impurities
  • Residue on ignition
  • Arsenic
  • Heavy metals
  • Loss on drying
  • Appearance
  • Physical-property characterization

For a pharmaceutical API page, the USP values should take priority over generic commercial CoA specifications when the two differ.

Storage

Oxaprozin should be stored in tight, light-resistant containers under controlled room-temperature conditions.

Because oxaprozin is light sensitive, protection from excessive light exposure is important during handling, sampling and storage.

Detailed Specifications

Parameter Specification
Appearance white to off-white crystalline powder
Identification IR & HPLC compliant
Assay (HPLC) 98.0% – 102.0%
Loss on Drying NMT 0.3%
Residue on Ignition NMT 0.3%
Heavy Metals NMT 10 ppm
Water Content 162–163°C
Melting Point 162–163°C
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