Obeticholic Acid API Manufacturer India

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Obeticholic Acid API Overview

Obeticholic Acid is a semi-synthetic bile acid derivative and potent farnesoid X receptor (FXR) agonist. It is structurally related to chenodeoxycholic acid and contains an additional ethyl group at the 6α-position.

Obeticholic Acid is an important pharmaceutical research compound associated with bile acid metabolism, hepatobiliary disorders, FXR signaling, liver disease research, and metabolic pathway studies.

The compound is also known as 6-Ethylchenodeoxycholic Acid, 6α-Ethylchenodeoxycholic Acid, 6-ECDCA, and INT-747. Its chemical formula is C₂₆H₄₄O₄, with a molecular weight of 420.63 g/mol.

Obeticholic Acid has been developed as an oral pharmaceutical active ingredient. It has been extensively studied for its ability to activate FXR, a nuclear receptor involved in bile acid homeostasis and several metabolic, inflammatory, and fibrotic pathways.

For pharmaceutical development and API manufacturing in India, Obeticholic Acid is listed commercially by Indian API companies, demonstrating established interest in the molecule within the Indian pharmaceutical manufacturing sector.

Chemical Information

  • Product Name: Obeticholic Acid
  • CAS Number: 459789-99-2
  • Molecular Formula: C₂₆H₄₄O₄
  • Molecular Weight: 420.63 g/mol
  • IUPAC Name: (4R)-4-[(3R,5S,6R,7R,8S,9S,10S,13R,14S,17R)-6-ethyl-3,7-dihydroxy-10,13-dimethyl...]-pentanoic acid
  • Chemical Name: 3α,7α-Dihydroxy-6α-ethyl-5β-cholan-24-oic acid
  • Alternative Names: 6-Ethylchenodeoxycholic Acid; 6α-Ethylchenodeoxycholic Acid; 6-ECDCA; INT-747
  • PubChem CID: 447715
  • UNII: 0462Z4S4OZ
  • ChEBI ID: CHEBI:43602
  • ChEMBL ID: CHEMBL566315
  • DrugBank ID: DB05990
  • Drug Class: Farnesoid X Receptor Agonist
  • Therapeutic Area: Hepatology / Gastroenterology
  • Molecule Type: Semi-Synthetic Small Molecule
  • Chemical Class: Bile Acid Derivative
  • Physical Form: White to off-white powder

The FDA substance record confirms the formula C₂₆H₄₄O₄ and molecular weight 420.63, while PubChem confirms CAS 459789-99-2 and the principal chemical identifiers.

Obeticholic Acid Mechanism of Action

Obeticholic Acid acts as an agonist of the farnesoid X receptor (FXR).

FXR is a nuclear receptor that plays a central role in regulating bile acid homeostasis. Activation of FXR influences gene expression involved in bile acid synthesis, transport, metabolism, and related hepatic pathways.

Obeticholic Acid-mediated FXR activation can influence:

  • Bile acid synthesis
  • Bile acid transport
  • Hepatic metabolism
  • Cholesterol metabolism
  • Lipid metabolism
  • Inflammatory signaling
  • Fibrotic pathways
  • Intestinal bile acid regulation

The FDA describes Obeticholic Acid as an FXR agonist and identifies FXR as a regulator of bile acid, inflammatory, fibrotic, and metabolic pathways.

Pharmaceutical Applications

Obeticholic Acid is used in pharmaceutical development and research involving FXR-mediated biological pathways.

Important application areas include:

  • FXR agonist drug development
  • Hepatobiliary pharmaceutical research
  • Bile acid metabolism research
  • Liver disease research
  • Cholestatic liver disease research
  • Fibrosis-related research
  • Metabolic pathway research
  • Pharmaceutical formulation development
  • Analytical method development
  • Medicinal chemistry research
  • Drug discovery programs
  • Reference and research applications

Obeticholic Acid has historically been developed for primary biliary cholangitis (PBC) and has been studied in additional liver-related conditions.

Regulatory note: The FDA records the U.S. accelerated approval of Ocaliva for PBC as withdrawn effective November 24, 2025. Therefore, current regulatory status should be checked for the relevant market before making therapeutic approval claims.

Obeticholic Acid Physical Characteristics

Obeticholic Acid is described as a white to off-white powder. The FDA labeling states that it is soluble in methanol, acetone, and ethyl acetate, while its water solubility is pH-dependent. It is slightly soluble at low pH and very soluble at high pH.

Key Physical Characteristics

  • White to off-white powder
  • Semi-synthetic bile acid derivative
  • Steroidal small molecule
  • FXR agonist
  • pH-dependent aqueous solubility
  • Soluble in methanol
  • Soluble in acetone
  • Soluble in ethyl acetate
  • Poorer aqueous solubility under acidic conditions

Obeticholic Acid Manufacturing Process

Obeticholic Acid is a semi-synthetic small-molecule API manufactured through controlled chemical synthesis and purification processes.

A pharmaceutical manufacturing process generally includes:

  • Qualification of starting materials
  • Controlled chemical synthesis
  • Reaction monitoring
  • Intermediate isolation
  • Purification
  • Solvent exchange
  • Crystallization
  • Solid isolation
  • Controlled drying
  • Milling and particle-size adjustment where required
  • Identity testing
  • Assay determination
  • Related-substance analysis
  • Residual-solvent testing
  • Elemental-impurity assessment
  • Stability testing
  • Controlled packaging

Because Obeticholic Acid contains several stereogenic centers, appropriate process controls are important for maintaining the required stereochemical profile.

Obeticholic Acid Quality Control

Quality control of Obeticholic Acid should address identity, assay, purity, stereochemical characteristics, residual solvents, elemental impurities, physical properties, and stability.

Typical quality-control parameters include:

  • Identification by IR
  • Identification by HPLC/UPLC
  • Assay by validated HPLC/UPLC
  • Related substances
  • Individual impurities
  • Total impurities
  • Water content or loss on drying
  • Residual solvents
  • Elemental impurities
  • Specific optical rotation where applicable
  • Melting behavior
  • Particle-size distribution where applicable
  • Solid-state characterization where applicable
  • Stability testing

A validated chromatographic method can be used for quantitative assay and related-substance analysis according to the applicable API specification.

Obeticholic Acid Solubility

Obeticholic Acid demonstrates pH-dependent water solubility.

The FDA describes Obeticholic Acid as:

  • Soluble in methanol
  • Soluble in acetone
  • Soluble in ethyl acetate
  • Slightly soluble in water at low pH
  • Very soluble in water at high pH

This pH-dependent behavior is consistent with the molecule's carboxylic-acid functionality.

Obeticholic Acid Melting Point

Reported literature values place the melting behavior of Obeticholic Acid around 108–110°C. However, thermal behavior can depend on crystalline form and analytical conditions.

For this reason, melting point should preferably be treated as a characterization parameter rather than a universal release specification unless it is specifically defined in the applicable API specification.

Obeticholic Acid API Manufacturer India

India has an established pharmaceutical API manufacturing sector with companies commercially listing Obeticholic Acid. Indian API listings include Obeticholic Acid with the CAS number 459789-99-2, supporting the use of search terms such as Obeticholic Acid Manufacturer India, Obeticholic Acid API Manufacturer India, and Obeticholic Acid API India for pharmaceutical B2B visibility.

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Pharmaceutical Formulation Development

Obeticholic Acid has been developed for oral pharmaceutical formulations.

The FDA-approved Ocaliva product was supplied as 5 mg and 10 mg film-coated tablets containing Obeticholic Acid as the active ingredient.

Formulation-development considerations include:

  • Particle size
  • Solid-state characteristics
  • Crystalline form
  • Dissolution behavior
  • pH-dependent solubility
  • Excipient compatibility
  • Chemical stability
  • Moisture sensitivity
  • Content uniformity
  • Bioavailability considerations

Obeticholic Acid in Pharmaceutical Research

Obeticholic Acid is an important research molecule for studying FXR-mediated pathways.

Research applications include:

  • FXR receptor research
  • Bile acid signaling studies
  • Hepatic metabolism research
  • Cholestatic liver disease research
  • Liver fibrosis research
  • Metabolic disease research
  • Inflammatory pathway research
  • Drug discovery
  • Medicinal chemistry
  • Pharmaceutical formulation research
  • Analytical method development

Storage and Handling

Obeticholic Acid API should be stored according to the validated API specification and available stability data.

Recommended general handling practices include:

  • Store in a tightly closed container
  • Protect from excessive moisture
  • Protect from direct light where required
  • Maintain controlled storage conditions
  • Minimize unnecessary environmental exposure
  • Use suitable moisture-protective packaging
  • Follow validated handling procedures

The specific storage temperature for API material should be established from the applicable stability data and approved product specification rather than assigning an unsupported universal temperature.

Key Features of Obeticholic Acid API

  • Semi-synthetic bile acid derivative
  • CAS Number 459789-99-2
  • Molecular formula C₂₆H₄₄O₄
  • Molecular weight 420.63 g/mol
  • Potent FXR agonist
  • Steroidal small molecule
  • Used in hepatobiliary research
  • Relevant to bile acid metabolism research
  • Suitable for pharmaceutical formulation development
  • pH-dependent aqueous solubility
  • White to off-white powder
  • Multiple stereocenters
  • Commercially listed by Indian API manufacturers

Detailed Specifications

Parameter Specification
Appearance White crystalline powder or crystals
Identification IR & HPLC compliant
Assay (HPLC) 98.0% – 102.0%
Loss on Drying NMT 1.0%
Residue on Ignition NMT 0.5%
Individual Impurity NMT 0.15%
Total Impurities NMT 2.0%
Water Content NMT 1.0%
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