Nisoldipine API Manufacturer in India

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Nisoldipine API

Nisoldipine is a synthetic 1,4-dihydropyridine calcium channel blocker and pharmaceutical active ingredient. It primarily acts on vascular smooth muscle by inhibiting L-type calcium channels, reducing calcium influx and producing vasodilation. Nisoldipine is associated with the management of hypertension and cardiovascular conditions requiring calcium-channel blockade.

Nisoldipine is a small-molecule API with the molecular formula C₂₀H₂₄N₂O₆ and molecular weight 388.4 g/mol.

Nisoldipine API Manufacturer in India

Nisoldipine is a specialized cardiovascular pharmaceutical API used in the development and manufacture of pharmaceutical formulations.

Important quality attributes include identity, assay, related substances, water content, residual solvents, elemental impurities, stereochemical/solid-state characteristics and other applicable pharmaceutical quality parameters.

Chemical Information

CAS Number: 63675-72-9

Molecular Formula: C₂₀H₂₄N₂O₆

Molecular Weight: 388.40 g/mol

Chemical Name: 3-O-methyl 5-O-(2-methylpropyl) 2,6-dimethyl-4-(2-nitrophenyl)-1,4-dihydropyridine-3,5-dicarboxylate

IUPAC Name: Methyl 2-methylpropyl 2,6-dimethyl-4-(2-nitrophenyl)-1,4-dihydropyridine-3,5-dicarboxylate

Drug Class: Dihydropyridine Calcium Channel Blocker

Therapeutic Class: Antihypertensive / Cardiovascular Agent

Therapeutic Area: Cardiovascular

Molecule Type: Synthetic Small Molecule

Development Code: BAY K 5552

PubChem confirms CAS 63675-72-9, molecular formula C₂₀H₂₄N₂O₆ and molecular weight 388.4 g/mol.

Mechanism of Action

Nisoldipine acts primarily by inhibiting L-type calcium channels in vascular smooth muscle.

Its pharmacological effects include:

  • Inhibition of voltage-gated L-type calcium channels
  • Reduction of calcium influx into vascular smooth muscle
  • Relaxation of vascular smooth muscle
  • Reduction of peripheral vascular resistance
  • Vasodilation
  • Reduction of arterial blood pressure

Nisoldipine is classified as a dihydropyridine calcium channel blocker.

Pharmaceutical Applications

Nisoldipine API is relevant to:

  • Antihypertensive formulation development
  • Cardiovascular drug development
  • Calcium channel blocker formulations
  • Extended-release tablet development
  • Pharmaceutical research
  • Cardiovascular pharmacology
  • Analytical research
  • Formulation development
  • Quality-control testing
  • Pharmaceutical manufacturing

Cardiovascular Applications

Nisoldipine is used as a calcium channel blocker in the management of hypertension. It has also been associated with treatment of angina pectoris in pharmacological references.

The current approved therapeutic use should always be determined according to the applicable regulatory labeling and jurisdiction.

Physical Characteristics

Nisoldipine is described as a yellow crystalline powder or yellow crystalline substance. It is practically insoluble in water and soluble in organic solvents including ethanol; some official labeling also reports solubility in acetone and methanol.

Solubility

Nisoldipine is practically insoluble in water and soluble in ethanol. Official labeling also describes solubility in acetone and methanol.

Manufacturing Process

A controlled Nisoldipine API manufacturing process may involve:

  1. Qualification of starting materials
  2. Preparation of substituted dihydropyridine intermediates
  3. Controlled chemical synthesis
  4. Esterification and functional-group transformations
  5. Reaction monitoring
  6. Purification
  7. Crystallization
  8. Filtration and washing
  9. Controlled drying
  10. Particle-size control, where applicable
  11. Final analytical testing
  12. GMP-compliant packaging

Quality Control Testing

Typical Nisoldipine API testing may include:

  • Identification by IR
  • HPLC identification
  • Assay by HPLC
  • Related substances
  • Individual impurities
  • Total impurities
  • Water content
  • Residual solvents
  • Elemental impurities
  • Solid-state characterization
  • Particle-size distribution, where applicable
  • Stability testing

Detailed Specifications

Parameter Specification
Appearance White crystalline powder or crystals
Identification IR & HPLC compliant
Assay (HPLC) 98.0% – 102.0%
Loss on Drying NMT 1.0%
Residue on Ignition NMT 0.5%
Individual Impurity NMT 0.5%
Total Impurities NMT 1.0%
Water Content NMT 1.0%
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