Nirogacestat API Manufacturer in India

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Nirogacestat API

Nirogacestat is a synthetic gamma-secretase inhibitor and an orally active small-molecule pharmaceutical ingredient. It inhibits gamma-secretase, an enzyme complex involved in the proteolytic processing of several transmembrane proteins, including the Notch receptor.

Nirogacestat is used as an active pharmaceutical ingredient in the development and manufacture of targeted oncology medicines, particularly for progressing desmoid tumors requiring systemic treatment. The marketed pharmaceutical form is nirogacestat hydrobromide (dihydrobromide). (dailymed.nlm.nih.gov)

Nirogacestat API Manufacturer in India

Nirogacestat is a specialized oncology pharmaceutical API used for gamma-secretase inhibition research, pharmaceutical formulation development and manufacture of targeted anticancer medicines.

The free base and pharmaceutical hydrobromide salt should be distinguished when preparing API documentation. FDA identifies the active ingredient in OGSIVEO as nirogacestat hydrobromide, while FDA's substance database separately identifies the free-base nirogacestat. (precision.fda.gov)

Chemical Information

CAS Number — Nirogacestat: 1290543-63-3

CAS Number — Nirogacestat Hydrobromide: 1962925-29-6

Molecular Formula — Nirogacestat: C₂₇H₄₁F₂N₅O

Molecular Weight — Nirogacestat: 489.64 g/mol

Molecular Formula — Nirogacestat Hydrobromide: C₂₇H₄₃Br₂F₂N₅O

Molecular Weight — Nirogacestat Hydrobromide: 651.48 g/mol

Chemical Name: (S)-2-(((S)-6,8-difluoro-1,2,3,4-tetrahydronaphthalen-2-yl)amino)-N-(1-(2-methyl-1-(neopentylamino)propan-2-yl)-1H-imidazol-4-yl)pentanamide dihydrobromide

Drug Class: Gamma-Secretase Inhibitor

Therapeutic Class: Antineoplastic Agent

Therapeutic Area: Oncology

Molecule Type: Synthetic Small Molecule

Development Code: PF-03084014 / PF-3084014

Target: Gamma-Secretase

FDA and PubChem identify the free base as C₂₇H₄₁F₂N₅O with molecular weight approximately 489.6 g/mol, while FDA/DailyMed identifies the hydrobromide form used in OGSIVEO as C₂₇H₄₃Br₂F₂N₅O with molecular weight 651.48 g/mol. (pubchem.ncbi.nlm.nih.gov)

Mechanism of Action

Nirogacestat inhibits the gamma-secretase enzyme complex, thereby preventing cleavage and activation of Notch receptors.

Its mechanism includes:

  • Inhibition of gamma-secretase
  • Reduction of Notch receptor cleavage
  • Inhibition of Notch pathway activation
  • Modulation of Notch-dependent cellular signaling
  • Reduction of signaling associated with tumor-cell proliferation
  • Antineoplastic activity against susceptible tumor biology

The NCI identifies nirogacestat as a gamma-secretase inhibitor that blocks proteolytic activation of the Notch receptor. (cancer.gov)

Pharmaceutical Applications

Nirogacestat API is relevant to:

  • Desmoid tumor treatment formulations
  • Gamma-secretase inhibitor development
  • Notch signaling research
  • Oncology drug development
  • Targeted anticancer therapy
  • Pharmaceutical formulation development
  • Tumor biology research
  • Drug discovery research
  • Antineoplastic API development
  • Pharmaceutical analytical research

Oncology Applications

Nirogacestat is indicated for adult patients with progressing desmoid tumors who require systemic treatment. Desmoid tumors are locally aggressive soft-tissue tumors associated with dysregulated cellular signaling.

Its therapeutic activity is associated with inhibition of gamma-secretase and subsequent reduction of Notch pathway signaling. (cancer.gov)

Notch Pathway

The Notch signaling pathway regulates processes including cellular differentiation, proliferation and tissue development.

Gamma-secretase participates in the proteolytic activation of Notch receptors. By inhibiting gamma-secretase, Nirogacestat interferes with Notch signaling and downstream biological processes relevant to desmoid tumor growth.

Physical Characteristics

Nirogacestat hydrobromide is described as a white to off-white powder. FDA/DailyMed reports a molecular weight of 651.48 g/mol for the dihydrobromide salt. (dailymed.nlm.nih.gov)

Solubility

Nirogacestat hydrobromide has an aqueous solubility of approximately 11.4 mg/mL at 25°C, with a measured aqueous solution pH of approximately 4.4. FDA/DailyMed notes that the dihydrobromide salt is highly soluble at low pH, while its solubility decreases substantially at pH values above 6.0. (dailymed.nlm.nih.gov)

pKa

Nirogacestat hydrobromide has reported pKa values of approximately:

  • pKa 1: 5.77
  • pKa 2: 7.13

These values help explain the pH-dependent aqueous solubility of the compound. (dailymed.nlm.nih.gov)

Manufacturing Process

A controlled Nirogacestat API manufacturing process may involve:

  1. Qualification of starting materials
  2. Preparation of substituted tetrahydronaphthalene intermediates
  3. Synthesis of the chiral amino-acid-derived intermediate
  4. Preparation of substituted imidazole intermediates
  5. Controlled coupling reactions
  6. Formation of Nirogacestat free base
  7. Purification
  8. Formation of the hydrobromide salt
  9. Controlled crystallization
  10. Filtration and washing
  11. Controlled drying
  12. Particle-size control, where applicable
  13. Final analytical testing
  14. GMP-compliant packaging

Quality Control Testing

Typical Nirogacestat Hydrobromide API testing may include:

  • Identification by IR
  • HPLC identification
  • Assay by HPLC
  • Related substances
  • Individual impurities
  • Total impurities
  • Water content
  • Residual solvents
  • Elemental impurities
  • Chiral purity
  • Solid-state characterization
  • Particle-size distribution
  • pH of specified solution
  • Stability testing

Detailed Specifications

Parameter Specification
Appearance White crystalline powder or crystals
Identification IR & HPLC compliant
Assay (HPLC) 98.0% – 102.0%
Loss on Drying NMT 1.0%
Residue on Ignition NMT 0.5%
Individual Impurity NMT 0.5%
Total Impurities NMT 1.0%
Water Content NMT 1.0%
Solubility 11.4 mg/mL in water at 25°C for Nirogacestat Hydrobromide
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