Nicardipine Hydrochloride API Manufacturer in India

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Nicardipine Hydrochloride API

Nicardipine Hydrochloride is a synthetic dihydropyridine calcium channel blocker and active pharmaceutical ingredient (API). It inhibits calcium ion influx through L-type calcium channels and produces vasodilation, particularly in arterial vascular smooth muscle.

Nicardipine Hydrochloride is used in pharmaceutical formulations for the management of hypertension and in clinical settings requiring controlled reduction of blood pressure. It is also used in pharmaceutical research and formulation development. Official FDA labeling identifies Nicardipine Hydrochloride as a calcium ion influx inhibitor.

Nicardipine Hydrochloride API Manufacturer in India

Nicardipine Hydrochloride is an established cardiovascular pharmaceutical API used in the development and manufacture of antihypertensive formulations.

USP defines Nicardipine Hydrochloride as containing NLT 98.0% and NMT 102.0% of nicardipine hydrochloride, calculated on the dried basis.

Chemical Information

CAS Number: 54527-84-3

Molecular Formula: C₂₆H₂₉N₃O₆·HCl

Molecular Weight: 515.99 g/mol

Free Base CAS: 55985-32-5

Free Base Molecular Weight: 479.53 g/mol

Chemical Name: 2-(Benzylmethylamino)ethyl methyl 1,4-dihydro-2,6-dimethyl-4-(3-nitrophenyl)-3,5-pyridinedicarboxylate monohydrochloride

Drug Class: Dihydropyridine Calcium Channel Blocker

Therapeutic Class: Antihypertensive

Therapeutic Area: Cardiovascular

Molecule Type: Synthetic Small Molecule

USP confirms the molecular formula, molecular weight and CAS information for Nicardipine Hydrochloride.

Mechanism of Action

Nicardipine Hydrochloride is a calcium channel blocker that inhibits calcium influx through L-type calcium channels.

Its pharmacological effects include:

  • Inhibition of calcium ion influx
  • Relaxation of arterial vascular smooth muscle
  • Reduction of systemic vascular resistance
  • Arterial vasodilation
  • Reduction in blood pressure
  • Increased coronary blood flow

Official labeling describes Nicardipine Hydrochloride as a calcium ion influx inhibitor or slow-channel blocker.

Pharmaceutical Applications

Nicardipine Hydrochloride API is relevant to:

  • Antihypertensive formulations
  • Cardiovascular pharmaceutical development
  • Calcium channel blocker research
  • Hypertension treatment research
  • Injectable formulation development
  • Oral pharmaceutical formulations
  • Cardiovascular drug development
  • Pharmaceutical API manufacturing
  • Analytical quality control
  • Pharmaceutical research and development

Antihypertensive Applications

Nicardipine is used as an antihypertensive agent because of its ability to produce arterial vasodilation through calcium-channel blockade.

It is available in both oral and intravenous pharmaceutical formulations, with intravenous Nicardipine Hydrochloride used when controlled blood-pressure reduction is clinically required.

Calcium Channel Blocker Activity

Nicardipine belongs to the 1,4-dihydropyridine calcium channel blocker class.

Its vascular effects are primarily associated with inhibition of calcium entry into vascular smooth muscle cells, resulting in relaxation and reduced vascular resistance.

Physical Characteristics

Nicardipine Hydrochloride is described as a pale greenish-yellow crystalline powder. FDA labeling reports a melting point of approximately 169°C, while other current labeling gives a range of approximately 167–171°C. It is soluble in methanol, sparingly soluble in ethanol and slightly soluble in acetone, chloroform and water.

Solubility

Nicardipine Hydrochloride is:

  • Soluble in methanol
  • Sparingly soluble in ethanol
  • Slightly soluble in acetone
  • Slightly soluble in chloroform
  • Slightly soluble in water

These solubility characteristics are reported in official product labeling.

Manufacturing Process

A controlled Nicardipine Hydrochloride API manufacturing process may involve:

  1. Qualification of starting materials
  2. Preparation of substituted dihydropyridine intermediates
  3. Controlled esterification reactions
  4. Formation of the dihydropyridine ring system
  5. Introduction of the nitrophenyl group
  6. Incorporation of the benzylmethylaminoethyl side chain
  7. Reaction monitoring
  8. Purification
  9. Formation of the hydrochloride salt
  10. Crystallization
  11. Filtration and washing
  12. Controlled drying
  13. Final analytical testing
  14. GMP-compliant packaging

Quality Control Testing

Typical Nicardipine Hydrochloride API testing may include:

  • Identification by IR
  • HPLC identification
  • Assay
  • Related substances
  • Individual impurities
  • Total impurities
  • Loss on drying
  • Residue on ignition / sulfated ash
  • Residual solvents
  • Elemental impurities
  • Stability testing

The current USP monograph establishes an assay range of 98.0–102.0% on the dried basis.

Storage

Store Nicardipine Hydrochloride API in an airtight container protected from light under controlled pharmaceutical storage conditions.

Nicardipine Hydrochloride is light-sensitive, and commercial technical information recommends cool, dark storage.

Detailed Specifications

Parameter Specification
Appearance White crystalline powder or crystals
Identification IR & HPLC compliant
Assay (HPLC) 98.0% – 102.0%
Loss on Drying NMT 1.0%
Residue on Ignition NMT 0.1%
Individual Impurity NMT 0.5%
Total Impurities NMT 1.0%
Water Content NMT 1.0%
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