Netarsudil API Manufacturer in India

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Netarsudil API

Netarsudil is a synthetic Rho-associated protein kinase (ROCK) inhibitor and norepinephrine transporter inhibitor used as a pharmaceutical active pharmaceutical ingredient (API). It acts primarily on pathways involved in aqueous humor dynamics and is associated with the management of elevated intraocular pressure (IOP) in ophthalmic applications.

Netarsudil is an important ophthalmic pharmaceutical compound used in the development and manufacture of formulations for glaucoma and ocular hypertension.

Netarsudil API Manufacturer in India

Netarsudil is a specialized ophthalmic API relevant to glaucoma drug development, ocular pharmacology, pharmaceutical formulation research and analytical quality control.

The compound is commonly encountered in pharmaceutical development as Netarsudil Mesylate, the salt form used in ophthalmic drug products. FDA documentation identifies Netarsudil Mesylate as the drug substance for the approved ophthalmic product.

Chemical Information

CAS Number: 1254032-66-0

Molecular Formula: C₂₈H₂₇N₃O₃

Molecular Weight: 453.5 g/mol

IUPAC Name: [4-[(2S)-3-amino-1-(isoquinolin-6-ylamino)-1-oxopropan-2-yl]phenyl]methyl 2,4-dimethylbenzoate

Development Code: AR-13324 / AR-13324 free base

Drug Class: Rho Kinase Inhibitor

Therapeutic Class: Ophthalmic Antiglaucoma Agent

Therapeutic Area: Ophthalmology

Molecule Type: Synthetic Small Molecule

Primary Targets: ROCK and Norepinephrine Transporter (NET)

PubChem reports the molecular formula as C₂₈H₂₇N₃O₃ and molecular weight as 453.5 g/mol.

Mechanism of Action

Netarsudil acts as a ROCK inhibitor and also inhibits the norepinephrine transporter.

Its pharmacological effects include:

  • Inhibition of Rho-associated protein kinase
  • Modulation of trabecular meshwork cell contractility
  • Increased aqueous humor outflow through the trabecular pathway
  • Reduction of episcleral venous pressure
  • Inhibition of norepinephrine transporter activity
  • Reduction of aqueous humor production
  • Lowering of intraocular pressure

These mechanisms contribute to the IOP-lowering activity of netarsudil.

Pharmaceutical Applications

Netarsudil API is relevant to:

  • Glaucoma ophthalmic formulations
  • Ocular hypertension formulations
  • Antiglaucoma drug development
  • ROCK inhibitor research
  • Ophthalmic pharmaceutical development
  • Intraocular pressure research
  • Aqueous humor outflow research
  • Ocular pharmacology
  • Pharmaceutical formulation development
  • Pharmaceutical API manufacturing
  • Analytical and quality-control testing

Ophthalmic Applications

Netarsudil ophthalmic preparations are associated with reducing elevated intraocular pressure in patients with open-angle glaucoma or ocular hypertension.

Its dual pharmacological activity involving ROCK inhibition and norepinephrine transporter inhibition provides a mechanism for increasing aqueous humor outflow and reducing factors contributing to elevated IOP.

ROCK Inhibition

Rho-associated protein kinase is involved in cellular contractility and regulation of the trabecular meshwork.

Netarsudil inhibits ROCK signaling, promoting relaxation of the trabecular meshwork and facilitating trabecular aqueous humor outflow. This mechanism distinguishes netarsudil from many conventional glaucoma medications.

Physical Characteristics

Netarsudil free base has a molecular formula of C₂₈H₂₇N₃O₃ and molecular weight of 453.5 g/mol. PubChem reports an XLogP3-AA value of approximately 4.6 and topological polar surface area of approximately 94.3 Ų.

For pharmaceutical manufacturing, Netarsudil is commonly handled as Netarsudil Mesylate. FDA documentation describes Netarsudil Mesylate drug substance as a light yellow to white powder.

Manufacturing Process

A controlled Netarsudil API manufacturing process may involve:

  1. Qualification of starting materials
  2. Preparation of chiral amino-acid-derived intermediates
  3. Preparation of isoquinoline intermediates
  4. Formation of the amide linkage
  5. Preparation of substituted benzyl ester intermediates
  6. Controlled coupling reactions
  7. Stereochemical control
  8. Formation of the required pharmaceutical salt
  9. Purification
  10. Crystallization
  11. Filtration and washing
  12. Controlled drying
  13. Final analytical testing
  14. GMP-compliant packaging

Quality Control Testing

Typical Netarsudil Mesylate API testing may include:

  • Identification by FTIR
  • HPLC identification
  • Assay by HPLC
  • Chromatographic purity
  • Specified impurities
  • Total impurities
  • Residual solvents
  • Water content
  • Chiral purity
  • Elemental impurities
  • Stability testing

FDA quality documentation confirms that Netarsudil Mesylate drug substance specifications include identification by FTIR and HPLC, assay, chromatographic purity, total impurities, residual-solvent testing and water-content testing.

Storage

Store Netarsudil API in a tightly closed container under controlled pharmaceutical storage conditions, protected from excessive moisture, heat and direct light.

Commercial storage conditions should be based on validated stability data and the applicable API specification.

Detailed Specifications

Parameter Specification
Appearance White crystalline powder or crystals
Identification IR & HPLC compliant
Assay (HPLC) 98.0% – 102.0%
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