Miconazole Nitrate API Manufacturer in India

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Miconazole Nitrate API

Miconazole Nitrate is a synthetic imidazole antifungal API used in pharmaceutical formulations for the treatment of various fungal and yeast infections. It acts by interfering with the biosynthesis of ergosterol, an essential component of fungal cell membranes, resulting in disruption of membrane integrity and inhibition of fungal growth.

Miconazole Nitrate is widely associated with topical antifungal pharmaceutical formulations and is available as an active pharmaceutical ingredient for pharmaceutical manufacturing and formulation development.

Miconazole Nitrate API Manufacturer in India

Miconazole Nitrate is a specialized antifungal pharmaceutical API used in the development and manufacture of topical and other pharmaceutical preparations.

The USP-NF monograph specifies Miconazole Nitrate at 98.0%–102.0% on the dried basis. The USP also specifies limits for loss on drying and residue on ignition.

Chemical Information

CAS Number: 22832-87-7
Molecular Formula: C18H14Cl4N2O·HNO3
Molecular Formula (combined): C18H15Cl4N3O4
Molecular Weight: 479.14 g/mol
Drug Class: Imidazole Antifungal
Therapeutic Class: Antifungal Agent
Therapeutic Area: Dermatology / Gynecology / Infectious Diseases
Molecule Type: Synthetic Small Molecule

These identity and molecular data are consistent with PubChem and the USP monograph.

Mechanism of Action

Miconazole Nitrate inhibits fungal lanosterol 14α-demethylase, a cytochrome P450-dependent enzyme involved in ergosterol biosynthesis.

This results in:

  • Reduced ergosterol synthesis
  • Alteration of fungal cell-membrane structure
  • Increased membrane permeability
  • Disruption of fungal cellular functions
  • Inhibition of fungal growth

Pharmaceutical Applications

Miconazole Nitrate API is used in pharmaceutical development for:

  • Cutaneous fungal infections
  • Candidiasis
  • Dermatophytosis
  • Tinea infections
  • Athlete's foot
  • Ringworm
  • Jock itch
  • Vulvovaginal fungal infections
  • Other susceptible superficial fungal infections

Dosage Form Applications

Miconazole Nitrate is used in formulations such as:

  • Creams
  • Ointments
  • Lotions
  • Powders
  • Vaginal creams
  • Vaginal preparations
  • Topical gels
  • Other antifungal pharmaceutical formulations

Physical Characteristics

Miconazole Nitrate is described pharmacopeially as a white or practically white crystalline powder. The USP-related description reports a melting range of approximately 178–183°C with decomposition.

Manufacturing Process

A controlled Miconazole Nitrate API manufacturing process may involve:

  1. Qualification of starting materials
  2. Preparation of miconazole intermediate
  3. Controlled chemical synthesis
  4. Purification
  5. Formation of the nitrate salt
  6. Crystallization
  7. Filtration
  8. Washing
  9. Controlled drying
  10. Milling or sieving where required
  11. Final analytical testing
  12. Pharmaceutical-grade packaging

Quality Control Testing

Miconazole Nitrate API quality control may include:

  • Identification by IR
  • HPLC identification
  • Assay
  • Related substances
  • Loss on drying
  • Residue on ignition
  • Optical rotation
  • Residual solvents
  • Elemental impurities
  • Melting range
  • Stability testing

The current USP monograph specifies loss on drying NMT 0.5% and residue on ignition NMT 0.2%. It also specifies optical rotation of −0.10° to +0.10° at 20°C under the stated test conditions.

Storage

The USP specifies that Miconazole Nitrate should be preserved in well-closed containers, protected from light, and stored at controlled room temperature.

Pharmaceutical Research

Miconazole Nitrate is relevant to research involving:

  • Antifungal drug development
  • Imidazole antifungals
  • Ergosterol biosynthesis
  • Fungal cell membranes
  • Candida species
  • Dermatophytes
  • Topical pharmaceutical formulations
  • Antimicrobial formulation research

Miconazole Nitrate API Summary

Miconazole Nitrate is an imidazole-class antifungal API with CAS Number 22832-87-7, molecular weight 479.14 g/mol, and a USP assay specification of 98.0%–102.0% on the dried basis. It is primarily used in pharmaceutical formulations for topical treatment of susceptible fungal and yeast infections.

Detailed Specifications

Parameter Specification
Appearance White crystalline powder or crystals
Identification IR & HPLC compliant
Assay (HPLC) 98.0% – 102.0%
Loss on Drying NMT 0.5%
Residue on Ignition NMT 0.2%
Heavy Metals NMT 10 ppm
Individual Impurity NMT 0.5%
Total Impurities NMT 1.0%
Water Content NMT 0.5%
Melting Point 178–183°C
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