Lidocaine HCl API Manufacturer in India

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Lidocaine HCl API

Lidocaine Hydrochloride, also known as Lidocaine HCl or Lignocaine Hydrochloride, is the hydrochloride salt of lidocaine and a widely used amide-type local anesthetic. It produces reversible blockade of nerve conduction and is used in pharmaceutical formulations for local and regional anesthesia. Lidocaine also has Class IB antiarrhythmic activity when administered systemically.

Lidocaine HCl works primarily by blocking voltage-gated sodium channels in nerve membranes. This reduces sodium-ion influx and prevents the initiation and propagation of action potentials, resulting in reversible loss of sensation.

Lidocaine HCl API Manufacturer in India

Lidocaine HCl is an established local anesthetic pharmaceutical API manufactured through controlled chemical synthesis, purification, hydrochloride salt formation and crystallization.

Important quality attributes include identity, assay, related substances, water content, pH, heavy metals, sulfated ash and residual solvents.

Chemical Information

CAS Number: 6108-05-0
Alternate / Anhydrous CAS: 73-78-9
Molecular Formula: C14H22N2O·HCl·H2O
Molecular Weight: 288.81 g/mol
Anhydrous Molecular Weight: 270.80 g/mol
Chemical Name: 2-(Diethylamino)-N-(2,6-dimethylphenyl)acetamide hydrochloride monohydrate
Synonyms: Lidocaine Hydrochloride, Lidocaine HCl, Lignocaine Hydrochloride, Xylocaine Hydrochloride
Drug Class: Local Anesthetic
Pharmacological Class: Amide Local Anesthetic / Class IB Antiarrhythmic
Therapeutic Area: Anesthesiology / Pain Management / Cardiology

Mechanism of Action

Lidocaine HCl blocks voltage-gated sodium channels in neuronal membranes. By reducing sodium permeability, it inhibits the generation and propagation of action potentials along nerves and produces reversible local anesthesia.

Pharmaceutical Applications

Lidocaine HCl is used in pharmaceutical formulations for:

  • Local anesthesia
  • Regional anesthesia
  • Infiltration anesthesia
  • Nerve blocks
  • Topical anesthesia
  • Dental anesthesia
  • Mucosal anesthesia
  • Pain management
  • Antiarrhythmic therapy

Lidocaine hydrochloride injection is used for infiltration and nerve-block procedures, while intravenous formulations are also used as antiarrhythmic therapy.

Physical Characteristics

Lidocaine Hydrochloride Monohydrate is a white or almost white crystalline powder, very soluble in water and freely soluble in ethanol. Published EP-grade specifications describe a melting point of 74–79°C for the monohydrate.

Manufacturing Process

A controlled Lidocaine HCl API manufacturing process may include:

  1. Preparation of qualified starting materials
  2. Synthesis of the lidocaine free-base intermediate
  3. Purification
  4. Controlled hydrochloride salt formation
  5. Crystallization
  6. Filtration
  7. Washing
  8. Drying under controlled conditions
  9. Milling, where required
  10. Final analytical testing
  11. GMP-compliant packaging

Quality Control Testing

Typical Lidocaine HCl API testing includes:

  • Identification by IR
  • Identification by chemical reactions
  • Assay by HPLC
  • Related substances
  • Appearance of solution
  • pH
  • Water content
  • Sulfated ash
  • Heavy metals
  • Residual solvents
  • Melting point
  • Stability testing

Storage

Store Lidocaine HCl in a tightly closed container under controlled pharmaceutical storage conditions, protected from excessive moisture, heat and direct light. Final storage requirements should follow the approved API specification and validated stability data.

Pharmaceutical Research

Lidocaine HCl is relevant to research involving:

  • Local anesthetics
  • Voltage-gated sodium channels
  • Nerve conduction
  • Regional anesthesia
  • Dental anesthesia
  • Topical anesthetics
  • Pain management
  • Antiarrhythmic agents
  • Class IB antiarrhythmics
  • Pharmaceutical formulation development

Detailed Specifications

Parameter Specification
Appearance White to off-white crystalline powder
Identification IR & HPLC compliant
Assay (HPLC) 98.0% – 102.0%
Loss on Drying NMT 1.0%
Residue on Ignition NMT 0.1%
pH (1% Solution) 4.0 – 5.5
Individual Impurity NMT 0.10%
Total Impurities NMT 5.0%
Water Content 5.5% – 7.0%
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