Ledipasvir API | HCV NS5A Inhibitor API Manufacturer in India

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Ledipasvir API

Ledipasvir is a potent, selective hepatitis C virus (HCV) NS5A inhibitor used as part of direct-acting antiviral (DAA) therapy for the treatment of chronic hepatitis C infection. It acts on the viral NS5A protein, which is essential for HCV RNA replication and viral assembly.

Ledipasvir is commonly combined with sofosbuvir in fixed-dose antiviral therapy for eligible patients with chronic HCV infection.

Ledipasvir API Manufacturer in India

Ledipasvir is a specialized antiviral pharmaceutical API requiring controlled multi-step chemical synthesis, purification and solid-state characterization.

Important quality attributes include identity, assay, related substances, stereochemical purity, water content, residual solvents, elemental impurities, polymorphic form and stability.

Chemical Information

CAS Number: 1256388-51-8
Molecular Formula: C49H54F2N8O6
Molecular Weight: 889.00 g/mol
Drug Class: Direct-Acting Antiviral
Pharmacological Class: HCV NS5A Inhibitor
Therapeutic Class: Antiviral Agent
Therapeutic Area: Hepatology / Infectious Diseases

Mechanism of Action

Ledipasvir selectively inhibits the HCV NS5A protein, a multifunctional viral protein required for efficient viral replication and assembly.

By interfering with NS5A function, ledipasvir:

  • Inhibits HCV RNA replication
  • Interferes with viral replication-complex function
  • Disrupts viral assembly processes
  • Reduces production of infectious HCV particles

Ledipasvir is generally used in combination with other direct-acting antivirals rather than as monotherapy.

Pharmaceutical Applications

Ledipasvir is used in combination antiviral regimens for the treatment of chronic hepatitis C virus infection.

It is particularly recognized as a component of the ledipasvir/sofosbuvir combination used in appropriate HCV patient populations.

Treatment suitability depends on factors such as HCV genotype, prior treatment history, liver status and applicable regulatory labeling.

NS5A Inhibitor Characteristics

Ledipasvir is a highly potent inhibitor of the HCV NS5A replication protein. NS5A inhibitors are an important component of modern DAA combinations because they target a viral protein distinct from the viral protease and polymerase.

Manufacturing Process

Typical API manufacturing may involve:

  1. Preparation of substituted aromatic and heterocyclic intermediates
  2. Controlled multi-step chemical synthesis
  3. Formation of key amide and carbamate linkages
  4. Introduction of fluorinated structural components
  5. Coupling of advanced intermediates
  6. Purification
  7. Crystallization
  8. Filtration
  9. Drying
  10. Final analytical testing
  11. Controlled packaging

Quality and Analytical Testing

Ledipasvir API quality evaluation may include:

  • Identification by IR
  • Identification by HPLC
  • Mass spectrometry
  • Assay
  • Related substances
  • Stereochemical purity
  • Diastereomeric impurities
  • Water content
  • Residual solvents
  • Elemental impurities
  • Residue on ignition
  • Polymorphic-form characterization
  • Particle-size distribution where required
  • Stability testing

Storage

Ledipasvir should be stored in a tightly closed container under controlled pharmaceutical storage conditions, protected from excessive heat, moisture and direct light. Final storage requirements should be established through validated stability studies.

Pharmaceutical Research and Development

Ledipasvir is relevant to research involving:

  • Hepatitis C virus
  • HCV NS5A
  • Direct-acting antivirals
  • Viral RNA replication
  • Antiviral drug development
  • HCV combination therapy
  • Sofosbuvir/ledipasvir combinations
  • Infectious disease pharmacology
  • Hepatology
  • Viral resistance research

Detailed Specifications

Parameter Specification
Appearance White to off-white crystalline powder
Identification IR & HPLC compliant
Assay (HPLC) 98.0% – 102.0%
Loss on Drying NMT 2.0%
Residue on Ignition NMT 0.5%
Heavy Metals NMT 10 ppm
pH (1% Solution) 2.0 – 4.0
Individual Impurity NMT 0.5%
Total Impurities ≤ 1.5%
Water Content NMT 1.0%
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