Lapatinib Ditosylate API | HER2/EGFR Tyrosine Kinase Inhibitor API Manufacturer in India

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Lapatinib Ditosylate API

Lapatinib Ditosylate is the ditosylate salt form of lapatinib, an orally active small-molecule tyrosine kinase inhibitor (TKI). Lapatinib selectively inhibits the intracellular kinase domains of HER2/ErbB2 and EGFR/ErbB1, interfering with receptor signaling involved in cancer-cell proliferation and survival.

Lapatinib Ditosylate is primarily associated with the pharmaceutical treatment of HER2-positive breast cancer in approved clinical settings.

Lapatinib Ditosylate API Manufacturer in India

Lapatinib Ditosylate is a specialized oncology pharmaceutical API manufactured through controlled chemical synthesis, purification and salt formation.

Important quality attributes include identity, assay, related substances, water content, residual solvents, elemental impurities, salt composition, polymorphic form and stability.

Chemical Information

CAS Number: 388082-78-8
Molecular Formula: C29H26ClFN4O4S · 2C7H8O3S
Molecular Weight: 925.45 g/mol
Drug Class: Antineoplastic Agent
Pharmacological Class: Tyrosine Kinase Inhibitor
Therapeutic Class: Anticancer / Targeted Therapy
Therapeutic Area: Oncology

Mechanism of Action

Lapatinib Ditosylate provides lapatinib, which reversibly inhibits the intracellular tyrosine kinase domains of:

  • HER2/ErbB2
  • EGFR/ErbB1

Blocking these receptors interferes with downstream signaling pathways involved in tumor-cell growth and survival.

Pharmaceutical Applications

Lapatinib Ditosylate is used in approved settings for:

  • HER2-positive advanced or metastatic breast cancer
  • Selected HER2-positive breast cancer treatment regimens
  • Combination therapy with other anticancer agents

The specific indication and combination depend on the applicable regulatory labeling.

Ditosylate Salt Characteristics

Lapatinib Ditosylate is formed by combining lapatinib with two molecules of p-toluenesulfonic acid (tosylate). The salt form is used as the pharmaceutical active ingredient in marketed lapatinib formulations.

Manufacturing Process

Typical API manufacturing may involve:

  1. Preparation of lapatinib intermediates
  2. Controlled chemical synthesis
  3. Purification of lapatinib
  4. Preparation of the tosylate salt
  5. Controlled salt formation
  6. Crystallization
  7. Filtration
  8. Drying
  9. Milling where required
  10. Final analytical testing
  11. Controlled packaging

Quality and Analytical Testing

Lapatinib Ditosylate API quality evaluation may include:

  • Identification by IR
  • Identification by HPLC
  • Assay
  • Related substances
  • Organic impurities
  • Water content
  • Residual solvents
  • Elemental impurities
  • Tosylate content
  • Polymorphic-form characterization
  • Particle-size distribution where required
  • Stability testing

Storage

Lapatinib Ditosylate should be stored in a tightly closed container under controlled pharmaceutical storage conditions, protected from excessive heat, moisture and direct light. Final storage conditions should be established through validated stability studies.

Pharmaceutical Research and Development

Lapatinib Ditosylate is relevant to research involving:

  • HER2/ErbB2 signaling
  • EGFR/ErbB1 signaling
  • Tyrosine kinase inhibition
  • Targeted cancer therapy
  • Breast cancer
  • Oncology drug development
  • Receptor signaling
  • Combination anticancer therapy

Detailed Specifications

Parameter Specification
Appearance White to off-white crystalline powder
Identification IR & HPLC compliant
Assay (HPLC) 98.0% – 102.0%
Loss on Drying NMT 2.0%
Residue on Ignition NMT 0.5%
Individual Impurity NMT 0.5%
Total Impurities ≤ 1.5%
Water Content NMT 2.0%
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