Ipilimumab API | Anti-CTLA-4 Monoclonal Antibody API Manufacturer in India

Swapnroop Pharma · WHO-GMP Certified · +91 87670 62101

Ipilimumab API

Ipilimumab is a fully human IgG1 monoclonal antibody that targets cytotoxic T-lymphocyte-associated antigen 4 (CTLA-4), an immune checkpoint receptor expressed on activated T cells.

By blocking CTLA-4-mediated inhibitory signaling, ipilimumab enhances T-cell activation and proliferation, thereby strengthening the body's antitumor immune response. It is an important immune checkpoint inhibitor used in oncology.

Ipilimumab API Manufacturer in India

Ipilimumab is a specialized recombinant monoclonal antibody pharmaceutical ingredient manufactured using mammalian cell-culture technology.

Its quality control requires comprehensive characterization of biological attributes including identity, purity, aggregation, charge variants, glycosylation, molecular weight, potency, CTLA-4 binding activity, host-cell proteins, residual DNA, endotoxins and sterility.

Biological Information

CAS Number: 477202-00-9
Molecular Formula: C6500H10036N1732O2008S48
Molecular Weight: Approximately 148 kDa
Molecule Type: Fully Human Monoclonal Antibody
Drug Class: Immune Checkpoint Inhibitor
Pharmacological Class: Anti-CTLA-4 Monoclonal Antibody
Therapeutic Class: Antineoplastic / Immunotherapy
Therapeutic Area: Oncology

Mechanism of Action

Ipilimumab binds to CTLA-4 and prevents CTLA-4 from interacting with its ligands CD80 and CD86 on antigen-presenting cells.

This removes an inhibitory signal that normally limits T-cell activation. The resulting increase in T-cell activity can enhance recognition and destruction of tumor cells.

Ipilimumab therefore acts by modulating the immune system rather than directly attacking tumor cells.

Pharmaceutical Applications

Ipilimumab is used in approved oncology regimens for selected cancers, including:

  • Melanoma
  • Renal cell carcinoma
  • Colorectal cancer with specified molecular characteristics
  • Hepatocellular carcinoma
  • Non-small cell lung cancer
  • Malignant pleural mesothelioma
  • Esophageal cancer
  • Other cancers in specific combination regimens

Approved indications and combinations depend on the applicable regulatory authorization.

Immune Checkpoint Inhibition

CTLA-4 is an important negative regulator of T-cell responses. By inhibiting CTLA-4, ipilimumab can enhance immune activation against malignant cells.

This mechanism represents a fundamental approach in modern cancer immunotherapy and differs from conventional cytotoxic chemotherapy.

Recombinant Manufacturing

Manufacturing of ipilimumab generally involves:

  1. Recombinant antibody expression
  2. Mammalian cell culture
  3. Harvest and clarification
  4. Protein recovery
  5. Chromatographic purification
  6. Viral clearance
  7. Concentration and buffer exchange
  8. Final polishing
  9. Formulation
  10. Sterile filtration
  11. Aseptic filling

Quality and Analytical Testing

Ipilimumab quality evaluation may include:

  • Identity testing
  • Protein concentration
  • Purity
  • Size-exclusion chromatography
  • Aggregate analysis
  • Charge-variant analysis
  • Peptide mapping
  • Glycosylation characterization
  • Molecular-weight determination
  • CTLA-4 binding activity
  • Biological potency
  • Host-cell protein testing
  • Residual host-cell DNA
  • Residual Protein A
  • Bacterial endotoxins
  • Bioburden
  • Sterility
  • Subvisible particles

Storage

Ipilimumab drug substance and finished pharmaceutical products should be stored according to validated stability data and approved product requirements. Appropriate temperature control is essential to maintain antibody structure, purity and biological activity.

Pharmaceutical Research and Development

Ipilimumab is relevant to research involving:

  • CTLA-4 biology
  • Immune checkpoint inhibition
  • T-cell activation
  • Cancer immunotherapy
  • Monoclonal antibody therapeutics
  • Tumor immunology
  • Combination immunotherapy
  • Recombinant antibody manufacturing

Ipilimumab API Summary

Ipilimumab is a fully human IgG1 monoclonal antibody targeting CTLA-4. It has CAS Number 477202-00-9 and an approximate molecular weight of 148 kDa. By blocking CTLA-4-mediated immune inhibition, ipilimumab enhances T-cell activation and is used as an immune checkpoint inhibitor in the treatment of selected cancers.

Detailed Specifications

Parameter Specification
Appearance White to off-white crystalline powder
Identification IR & HPLC compliant
Assay (HPLC) 98.0% – 102.0%
Loss on Drying NMT 1.0%
Residue on Ignition NMT 0.5%
Heavy Metals NMT 10 ppm
pH (1% Solution) 4.0 – 7.0
Water Content NMT 0.5%
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